Application of Fourier Transform Infrared Spectroscopy and X-Ray Diffraction in the Characterization of Bamboo Stalks

Authors

  • Onimi Ometere Ashama University of Benin, Benin City, Nigeria
  • Tina Ishioma Francis-Akilaki University of Benin, Benin City, Nigeria

DOI:

https://doi.org/10.38035/gijes.v4i1.734

Keywords:

Bamboo Stalks, Fourier Transform Infrared Spectroscopy, FTIR, Particleboard, Sustainable Materials, X-Ray Diffraction

Abstract

Bamboo stalks have recently attracted increasing attention as sustainable agricultural by-products because of their rapid growth cycle, self-regeneration ability, and low maintenance requirements. Bamboo is widely distributed across tropical and subtropical regions of Nigeria, with Oxytenanthera abyssinica being one of the most dominant species. In spite of its extensive use in construction and craft applications, the material potential of bamboo stalks for engineered wood products remains underexplored. This study investigates the suitability of bamboo stalks as an eco-friendly precursor for particleboard production using Fourier Transform Infrared Spectroscopy (FTIR) and X-ray Diffraction (XRD) methods. FTIR analysis result revealed that characteristic absorption bands associated with cellulose, hemicellulose, and lignin, with prominent peaks observed at 1737 cm⁻¹, 1511 cm⁻¹, and 1379 cm⁻¹. Also, XRD analysis result showed distinct diffraction maxima at 2θ angles of approximately 15° and 22°, indicative of a high degree of cellulose crystallinity. Chemical composition analysis established that the bamboo biomass contained 52.61% cellulose, 19.16% hemicellulose, and 24.27% lignin, with negligible amounts of extractives (2.21%) and ash (1.75%). The combined FTIR and XRD results prove that bamboo stalks possess favourable chemical and structural properties, supporting their potential application as sustainable raw materials for particleboard manufacturing.

References

Alemdar, A., and Sain, M. (2008). Isolation and characterization of nanofibers from agricultural residues–Wheat straw and soy hulls. Bioresource technology, 99(6), pp. 1664-1671.

Alencar, M. A. S., Rambo, M. K. D., Botelho, G. L. G. T., Barros, P. M. M., Sergio, R. L., Borges, M. S., and Bertuol, D. (2023). Feasibility study of incorporation of bamboo plant fibers in cement matrices. Sustainable Chemistry for the Environment, 2, 100020.

Amenaghawon, N. A., Osayuki-Aguebor, W. and Okieimen, C. O. (2016a). Production of particle boards from corn cobs and cassava stalks: Optimization of mechanical properties using response surface methodology. Journal of Materials and Environmental Sciences, 7(4), pp. 1236-1244.

Beriber, A., Berrama, T., Doufene, N., Zekkaoui, C., and Dadou, S. (2023). Use of desalination plant brine activated bamboo stalks as a novel biosorbent to dyestuff removal. Biomass Conversion and Biorefinery, 1-20.

Biswas, S., Rahaman, T., Gupta, P., Mitra, R., Dutta, S., Kharlyngdoh, E., and Das, M. (2022). Cellulose and lignin profiling in seven, economically important bamboo species of India by anatomical, biochemical, FTIR spectroscopy and thermogravimetric analysis. Biomass and Bioenergy, 158, p. 106362.

Cabalova, I., Krilek, J., Kačík, F., Lagaňa, R., and Jurczyková, T. (2023). Valorization of Wood-Based Waste from Grapevine. Forests, 14(3), p. 442.

Emenike E. C., Iwuozor K. O., Agbana S. A., Otoikhian K. S., and Adeniyi A. G. (2022) Efficient recycling of disposable face masks via co-carbonization with waste biomass: a pathway to a cleaner environment. Cleaner Environmental Systems, 6, 100094.

Essid, S., Hegde, V. J., Mahieu, A., Bizet, L., Leblanc, N., and Saouab, A. (2021). Comparison of the properties of flax shives based particleboards prepared using binders of bio-based lignin and partially bio-based epoxy resin. International Journal of Adhesion and Adhesives, 109, p. 102915.

Gautam N., Rajesh Y., Kale N., Jagtap M., Chaudhari H., and Pansare S. (2023) Silica extraction from bamboo leaves using alkaline extraction method. Materials Today: Proceedings.

Goh, Y., Yap, S. P., and Tong, T. Y. (2020). Bamboo: the emerging renewable material for sustainable construction. Encyclopedia of Renewable and Sustainable Materials, 2, 365-376.

Jakob, M., Mahendran, A. R., Gindl-Altmutter, W., Bliem, P., Konnerth, J., Mueller, U., and Veigel, S. (2022). The strength and stiffness of oriented wood and cellulose-fibre materials: A review. Progress in Materials Science, 125, 100916.

Kumar, R., Kumari, S., Surah, S. S., Rai, B., Kumar, R., Sirohi, S., and Kumar, G. (2019). A simple approach for the isolation of cellulose nanofibers from banana fibers. Materials Research Express, 6(10), p. 105601.

Lin, Q., Gao, R., Li, D., Lu, Y., Liu, S., Yu, Y., and Yu, W. (2022). Bamboo-inspired cell-scale assembly for energy device applications. npj Flexible Electronics, 6(1), p. 13.

Nwobi-Okoye, C. C., Anyichie, M. K. and Atuanya, C. U. (2020). RSM and ANN modeling for production of newbouldia laevies fibre and recycled high density polyethylene composite: multi objective optimization using genetic algorithm. Fibers and Polymers, 21(4), pp. 898-909.

Shu B., Xiao Z., Hong L., Zhang S., Li C., Fu N., and Lu X. (2020) Review of the application of bamboo-based materials in construction engineering. Journal of Renewable Materials, 8(10), 1215-1242.

Sluiter, A Hyman, D., Payne, C., and Wolfe, J. (2008c) Determination of Insoluble Solids in Pretreated Biomass Material, Laboratory Analytical Procedure, Technical Report NREL/TP-510-42627. Natl. Renew. Energy Lab.

Sluiter, A., Hames, B., Hyman, D., Payne, C., Ruiz, R., Scarlata, C., Sluiter, J., Templeton, D., and Wolfe, J. (2008a) Determination of Total Solids in Biomass and Total Dissolved Solids in Liquid Process Samples, Laboratory Analytical Procedure, Technical Report NREL/TP-510-42621. Natl. Renew. Energy Lab.

Sluiter, A., Hames, B., Ruiz, R., Scarlata, C., Sluiter, J., and Templeton, D. (2008b) Determination of Sugars, Byproducts, and Degradation Products in Liquid Fraction Process Samples, Laboratory Analytical Procedure, Technical Report NREL/TP-510-42623. Natl. Renew. Energy Lab.

Sluiter, A., Hames, B., Ruiz, R., Scarlata, C., Sluiter, J., Templeton, D., and Crocker, D. (2012) Determination of Structural Carbohydrates and Lignin in Biomass, Laboratory Analytical Procedure, Technical Report NREL/TP-510-42618. Natl. Renew. Energy Lab.

Younesi-Kordkheili, H., and Pizzi, A. (2023). Lignin-based wood adhesives: A comparison between the influence of soda and Kraft lignin. International Journal of Adhesion and Adhesives, 121, p. 103312.

Published

2026-04-22

How to Cite

Ashama, O. O., & Francis-Akilaki, T. I. (2026). Application of Fourier Transform Infrared Spectroscopy and X-Ray Diffraction in the Characterization of Bamboo Stalks. Greenation International Journal of Engineering Science, 4(1), 25–30. https://doi.org/10.38035/gijes.v4i1.734